Nonionic Superbase-Catalyzed Silylation of Alcohols
نویسندگان
چکیده
منابع مشابه
Silylation of Alcohols and Phenols Using HMDS Catalyzed by SiO2-Cl in Solution and Solvent-Free Conditions
Trimethylsilylation of a variety of alcohols and phenols, in the presence of silica chloride, using hexamethyldisilazane (HMDS) in solution and under solvent-free conditions is reported. Trimethylsilyl ethers were formed in excellent yields both for aliphatic alcohols and phenols without having an electron-withdrawing group. In addition, SiO2-Cl can be recovered and reused after drying.
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ژورنال
عنوان ژورنال: The Journal of Organic Chemistry
سال: 1998
ISSN: 0022-3263,1520-6904
DOI: 10.1021/jo9840123